
New TopShim run:

version = topshim 2.4.0
date = 2026-10-19
time = 19:13:25.990
command = topshim  convcomp ordmax=4

FINE SHIMMING

Parameters:

probe = Z104275_0310
solvent = CDCl3
shim nucleus = 2H
nucleus optimised for = 1H
o1p (from lock) = 7.24 ppm

Results:


1D Shimming:
Low S/N encountered. The acquisition parameters will be changed to improve this issue.
echo time must be reduced
Iteration  1: FWHM Before= 6.6 Hz, Target= 1.0 Hz, After= 1.2 Hz
Iteration  2: FWHM Before= 1.2 Hz, Target= 0.6 Hz, After= 0.3 Hz
Iteration  3: FWHM Before= 0.3 Hz, Target= 0.7 Hz, After= 1.2 Hz
Iteration  4: FWHM Before= 1.2 Hz, Target= 1.2 Hz, After= 1.1 Hz
Iteration  5: FWHM Before= 1.1 Hz, Target= 1.9 Hz, After= 1.5 Hz
Iteration  6: FWHM Before= 1.5 Hz, Target= 1.6 Hz, After= 1.9 Hz
Iteration  7: FWHM Before= 1.9 Hz, Target= 1.7 Hz, After= 0.2 Hz
Shim succeeded

Lineshape quality factor (1D spectrum, spinning) = 1.1

shim changes: 
Z	-3008
Z2	-6062
Z3	-15862
Z4	-25156

duration = 6 min 2 sec
completed successfully
finished Mon Oct 19 19:19:26 2026


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